X-ray investigation of cubic crystal structures / Debye-Scherrer powder method

Item No. P2541405 | Type: Experiments

45 Minutes
45 Minutes
University
Students
heavy
EUR 18,402.50
Content 1 piece
EUR 21,898.98 Incl. VAT

Principle

When polycrystalline samples are irradiated with X-rays a characteristic diffraction pattern results. These Debye-Scherrer reflections are photographed and then evaluated.

Tasks

  1. Debye-Scherrer photographs are to be taken of powdered samples of sodium chloride and caesium chloride.
  2. The Debye-Scherrer rings are to be evaluated and assigned to the corresponding lattice planes.
  3. The lattice constants of the sample materials are to be determined.
  4. The number of atoms in the unit cells of each sample are to be determined.

Learning objectives

  • Crystal lattices
  • Crystal systems
  • Reciprocal lattice
  • Miller indices
  • Structure amplitude
  • Atomic form factor
  • Bragg scattering

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(de) Versuchsbeschreibung
p2541401d .pdf
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(de) Versuchsbeschreibung_docx
p2541401d .docx
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(en) Versuchsbeschreibung
p2541405_en .pdf
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p2541405_es .pdf
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